HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 11500555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 69347014 | HCID 69347014 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11500555 | HCID 11500555 | — |
Reaction Steps
To 3-Allyl-5,8-dichloro-1,2,3,4-tetrahydro-cyclopenta[b]indole-3-carboxylic acid ethyl ester was added 1 mL of 2.0 M lithium hydroxide aqueous solution and 1 mL of ethanol. The reaction mixture was stirred at room temperature for 2 hours than concentrated. The residue was purified by reverse phase HPLC to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07250441B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-aa336a1547174ba7b2b96ac9670e5eab |
| Source note | uspto-grants-2007_07 |