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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1297263Generated: October 30, 2026

Lithium Hydroxide → HCID 11500555, compound

https://huagongshe.com/reaction/1297263

Reaction equation

Participants

RoleNameHCIDCharge
ReactantLithium HydroxideHCID 3939—
ReactantHCID 69347014HCID 69347014—
SolventEthanolHCID 702—
ProductHCID 11500555HCID 11500555—

Reaction Steps

To 3-Allyl-5,8-dichloro-1,2,3,4-tetrahydro-cyclopenta[b]indole-3-carboxylic acid ethyl ester was added 1 mL of 2.0 M lithium hydroxide aqueous solution and 1 mL of ethanol. The reaction mixture was stirred at room temperature for 2 hours than concentrated. The residue was purified by reverse phase HPLC to give the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07250441B2
Source datasetuspto-grants-2007_07
ORD IDord-aa336a1547174ba7b2b96ac9670e5eab
Source noteuspto-grants-2007_07