HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → 6-[2-amino-4-oxo-4H-thiazol-(5Z)-ylidenemethyl]-4-isobutyl-quinoline-3-carbonitrile methanesulfonic acid salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 6-[2-Amino-4-oxo-4h-thiazol-(5z)-ylidenemethyl]-4-isobutyl-quinoline-3-carbonitrile | HCID 11624191 | — |
| Product | 6-[2-amino-4-oxo-4H-thiazol-(5Z)-ylidenemethyl]-4-isobutyl-quinoline-3-carbonitrile methanesulfonic acid salt | HCID 131726541 | — |
Reaction Steps
Similar procedure as described in example 47 was used, starting from 6-[2-amino-4-oxo-4H-thiazol-(5Z)-ylidenemethyl]-4-isobutyl-quinoline-3-carbonitrile (example 46g) and methanesulfonic acid to give 6-[2-amino-4-oxo-4H-thiazol-(5Z)-ylidenemethyl]-4-isobutyl-quinoline-3-carbonitrile methanesulfonic acid salt. LC-MS m/e 337 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07250515B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-3bb8cd6e6fd242288a9e7ad44821bdde |
| Source note | uspto-grants-2007_07 |