HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 58585848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Lithium Chloride | HCID 433294 | — |
| Reactant | HCID 58585851 | HCID 58585851 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 58585848 | HCID 58585848 | — |
Reaction Steps
Similar procedure as described in example 71b was used, starting 2-(3-cyano-6-iodo-quinolin-4-yl)-malonic acid diethyl ester (example 73a), lithium chloride, water, and dimethylsulfoxide to give 6-iodo-4-methyl-quinoline-3-carbonitrile. LC-MS m/e 295 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07250515B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-37473fa5fe2c46139ad318560cf8a458 |
| Source note | uspto-grants-2007_07 |