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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1297737Generated: October 30, 2026

Methyl iodide → HCID 68825957, compound

https://huagongshe.com/reaction/1297737

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantDiisopropylethylamineHCID 81531—
ReactantHCID 76823851HCID 76823851—
SolventAcetonitrileHCID 6342—
ProductHCID 68825957HCID 68825957—

Reaction Steps

Similar procedure as described in example 41b was used, starting from 5-(4-ethoxy-3-methanesulfonyl-quinolin-6-ylmethylene)-2-thioxo-thiazolidin-4-one (example 74d), iodomethane, and DIEA (diisopropylethylamine) in acetonitrile to give 5-(4-ethoxy-3-methanesulfonyl-quinolin-6-ylmethylene)-2-ethylsulfanyl-thiazol-4-one. LC-MS m/e 409 (MH+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07250515B2
Source datasetuspto-grants-2007_07
ORD IDord-16b898fed852429e87cc0dcb02651de0
Source noteuspto-grants-2007_07