HCID 19370428, compound → HCID 19370455, compound

HRID 129780Notes

Reaction equation

HRID 129780 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9](=[O:19])[CH2:10][C:11]2[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][CH:12]=2)=[C:5]([S:20][CH3:21])[CH:4]=1>O1CCCC1>[OH:19][C:9]([C:6]1[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[CH:4][C:5]=1[S:20][CH3:21])([CH2:6][CH2:7][CH2:8][CH2:3][CH:4]=[CH2:5])[CH2:10][C:11]1[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][CH:12]=1

Participants

3

Reactant 1

HCID 19370428HCID 19370428, compound

Product 1

HCID 19370455HCID 19370455, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

In this case absolute tetrahydrofuran is used as the solvent for preparation of the Grignard reagent. 6-bromine-1-hexen and 1-(4-methoxy-2-methylthiophenyl)-2-(4-methoxyphenyl)ethanon (71) are used as educts.

Sources & evidence

ORD record
ord-78045b6f1d344adbb208698a61896fc8
Source dataset
uspto-grants-1995_11
Patent number
US05470854

Reaction notes

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