Iodo benzene diacetate → HCID 53750351, Verbindung

HRID 129964Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 129964
[NH:1]([C:23]([O:25][CH:26]1[CH2:31][C:30]([CH3:33])([CH3:32])[N:29]([O:34][CH:35]2[CH2:40][CH2:39][CH2:38][CH2:37][CH2:36]2)[C:28]([CH3:42])([CH3:41])[CH2:27]1)=[O:24])[NH:2][C:3]([O:5][CH:6]1[CH2:11][C:10]([CH3:13])([CH3:12])[N:9]([O:14][CH:15]2[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]2)[C:8]([CH3:22])([CH3:21])[CH2:7]1)=[O:4].C(O)(=O)C.C(O)(=O)C.IC1C=CC=CC=1>>[N:2]([C:3]([O:5][CH:6]1[CH2:7][C:8]([CH3:22])([CH3:21])[N:9]([O:14][CH:15]2[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]2)[C:10]([CH3:13])([CH3:12])[CH2:11]1)=[O:4])=[N:1][C:23]([O:25][CH:26]1[CH2:27][C:28]([CH3:41])([CH3:42])[N:29]([O:34][CH:35]2[CH2:36][CH2:37][CH2:38][CH2:39][CH2:40]2)[C:30]([CH3:32])([CH3:33])[CH2:31]1)=[O:24]

Komponenten

3

Edukt 2

HCID 12217721Iodo benzene diacetateHCID 54341087Bis(1-cyclohexyloxy-2,2,6,6-tetramethylpiperidin-4-yl) Hydrazine-1,2-dicarboxylate

Produkt 1

HCID 53750351HCID 53750351, VerbindungAusbeute 84,7 %

Versuchsvorschrift

The procedure of Example 4 is repeated using 12.2 g of bis(1-cyclohexyloxy-2,2,6,6-tetramethylpiperidin-4-yl) hydrazine-1,2-dicarboxylate and 7.2 g of iodobenzene diacetate to afford 10.3 g of the title compound; mp 189°-191 ° C.

Quellen und Nachweise

ORD-Eintrag
ord-26767bc030df4704a7f0c698a1efa7f5
Quelldatensatz
uspto-grants-1995_11
Patentnummer
US05470980

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