HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodo benzene diacetate → Bis(1-cyclohexyloxy-2,2,6,6-tetramethylpiperidin-4-yl) Azodicarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodo benzene diacetate | HCID 12217721 | — |
| Reactant | Bis(1-cyclohexyloxy-2,2,6,6-tetramethylpiperidin-4-yl) Hydrazine-1,2-dicarboxylate | HCID 54341087 | — |
| Product | Bis(1-cyclohexyloxy-2,2,6,6-tetramethylpiperidin-4-yl) Azodicarboxylate | HCID 53750351 | 84.7% |
Reaction Steps
The procedure of Example 4 is repeated using 12.2 g of bis(1-cyclohexyloxy-2,2,6,6-tetramethylpiperidin-4-yl) hydrazine-1,2-dicarboxylate and 7.2 g of iodobenzene diacetate to afford 10.3 g of the title compound; mp 189°-191 ° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05470980 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-26767bc030df4704a7f0c698a1efa7f5 |
| Source note | uspto-grants-1995_11 |