HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 18458085, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 5-(4,4,5,5,5-Pentafluoro-3-oxopentanoyl)thiophene-2-carbonitrile | HCID 18458086 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18458085 | HCID 18458085 | — |
Reaction Steps
A mixture of 1-(5-cyano-2-thienyl)-4,4,5,5,5-pentafluoro-1,3-pentanedione (0.78 g), sulfuric acid (9 ml) and acetic acid (10 ml) was refluxed for 2 hours. The cooled mixture was poured into 100 ml of water. The precipitation was filtered and washed with water. 1H NMR (CDCl3): 6.53 (s, 1 H); 7.57 (d, 1H, J=4.1 Hz); 7.78 (d, 1H, J=4.1 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07381567B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-69ceee4e75614818a57ad74fb53c4c15 |
| Source note | uspto-grants-2008_06 |