HRID130298

反应详情

EQUATION

反应方程式

HRID 130298 的结构方程式

PROCEDURE

实验过程

The compound was synthesized according to example 1 using 2-acetylnaphthalene and ethyl heptafluorobutyrate as starting materials. The product was crystallized from petroleum ether. 1H NMR (CDCl3): 6.76 (s, 1 H); 7.57-7.66 (m, 2H); 7.90 (bd, 1 H); 7.93-7.94 (m, 2H); 7.98 (bd, 1 H); 8.53 (s, 1H). IR (film): 1602 (C═O); 1232 (C—F).

WORKUP

后处理

  1. customThe compound was synthesized
  2. customThe product was crystallized from petroleum ether