HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetylnaphthalene → 4,4,5,5,6,6,6-Heptafluoro-1-(2-naphthyl)hexane-1,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetylnaphthalene | HCID 7122 | — |
| Reactant | Butanoic acid, 2,2,3,3,4,4,4-heptafluoro-, ethyl ester | HCID 9644 | — |
| Product | 4,4,5,5,6,6,6-Heptafluoro-1-(2-naphthyl)hexane-1,3-dione | HCID 86004327 | — |
Reaction Steps
The compound was synthesized according to example 1 using 2-acetylnaphthalene and ethyl heptafluorobutyrate as starting materials. The product was crystallized from petroleum ether. 1H NMR (CDCl3): 6.76 (s, 1 H); 7.57-7.66 (m, 2H); 7.90 (bd, 1 H); 7.93-7.94 (m, 2H); 7.98 (bd, 1 H); 8.53 (s, 1H). IR (film): 1602 (C═O); 1232 (C—F).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07381567B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-ed593dcb2091417f8386ebc40775ec71 |
| Source note | uspto-grants-2008_06 |