HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Pyridin-3-yl)ethan-1-amine → HCID 59729913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Pyridin-3-yl)ethan-1-amine | HCID 854051 | — |
| Reactant | 6-(4-Formyl-2-methoxyphenoxy)nicotinamide | HCID 59730016 | — |
| Product | HCID 59729913 | HCID 59729913 | 58.4% |
Reaction Steps
Using a method similar to Example 405, a reaction of 6-(4-formyl-2-methoxyphenoxy)nicotinamide (Example 414, Part B) (0.050 g, 0.184 mmol) and 2-(pyridin-3-yl)ethylamine (0.0224 g, 0.184 mmol) gives the title compound (0.0406 g, 58.4%): TOF MS ES+ 379.2 (M+H)+, HRMS calcd for C21H23N4O3 379.1770 (M+H)+, found 379.1759, time 0.41 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07381719B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-59e7830ccea34e46a963314b852e200d |
| Source note | uspto-grants-2008_06 |