Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(S)-1,4-Dibenzyl-2-(3-methoxy-allyl)-piperazine → (2S)-2-(3-Methoxypropyl)piperazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (S)-1,4-Dibenzyl-2-(3-methoxy-allyl)-piperazine | HCID 69210439 | — |
| 촉매 | Palladium hydroxide | HCID 9942167 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | (2S)-2-(3-Methoxypropyl)piperazine | HCID 45099475 | — |
반응 단계
Add 20% Pd(OH)2/C (2.15 g) to (S)-1,4-dibenzyl-2-(3-methoxy-allyl)-piperazine (3.382 g, 10.05 mmol) in ethanol (100 mL) and under hydrogen atmosphere at 40° C. over night. Filter to give the title compound: mass spectrum (m/e):159.1 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07384934B2 |
| 출처 데이터셋 | uspto-grants-2008_06 |
| ORD ID | ord-73b794978d3149baabc6f734f140d468 |
| 출처 메모 | uspto-grants-2008_06 |