HRID131409

反应详情

EQUATION

反应方程式

HRID 131409 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Add 20% Pd(OH)2/C (2.15 g) to (S)-1,4-dibenzyl-2-(3-methoxy-allyl)-piperazine (3.382 g, 10.05 mmol) in ethanol (100 mL) and under hydrogen atmosphere at 40° C. over night. Filter to give the title compound: mass spectrum (m/e):159.1 (M+1).

WORKUP

后处理

  1. waitunder hydrogen atmosphere at 40° C. over night
  2. filtrationFilter