HCID 135543774, compound → HCID 136384193, compound

Participants

Reaction Steps

Using a method similar to Example (S)-8-fluoro-2-trifluoromethyl-11-[3-(2-methoxy-ethyl)-4-methyl-piperazin-1-yl]-5H-dibenzo[b,e][1,4]diazepine succinate, using (S)-8-chloro-2-trifluoromethyl-11-[3-(2-methoxy-ethyl)-piperazin-1-yl]-5H-dibenzo[b,e][1,4]diazepine (0.051 g, 0.12 mmol) to give 0.054 g (100% yield) of the free base as a yellow oil which is converted to the succinate salt as described previously: Mass Spectrum (m/e): 454(M+1).

Provenance & Evidence