HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-2-(2-Methoxyethyl)piperazine → (S)-10-[3-(2-Methoxyethyl)piperazin-1-yl]-2-methyl-4H-3-thia-1,4,9-triazabenzo[f]azulene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-2-(2-Methoxyethyl)piperazine | HCID 55287560 | — |
| Reactant | 2-methyl-4H-3-thia-1,4,9-triazabenzo[f]azulene-10-ylamine hydrochloride | HCID 135797745 | — |
| Product | (S)-10-[3-(2-Methoxyethyl)piperazin-1-yl]-2-methyl-4H-3-thia-1,4,9-triazabenzo[f]azulene | HCID 135464220 | — |
Reaction Steps
In a manner such as that described in Example 300, combine 2-methyl-4H-3-thia-1,4,9-triazabenzo[f]azulene-10-ylamine hydrochloride (0.437 g, 1.64 mmol) and (S)-2-(2-methoxyethyl)piperazine (0.474 g, 3.29 mmol) to obtain the title compound: mass spectrum (APCI): m/z=358.0 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07384934B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-d03035609b3a4f65bcaefcbfe3bfc5ab |
| Source note | uspto-grants-2008_06 |