Hydrochloric Acid → HCID 68804457, compound

Participants

Reaction Steps

Sodium hydroxide (0.8 ml, 1M) was added to a solution of the product of example 37 part b) (190 mg) in tetrahydrofuran under nitrogen. Methanol was added to solubilise the solution and the reaction mixture was stirred at room temperature for 3 hours. HCl (0.4 ml, 2M) was added to neutralise the solution and the mixture was concentrated in vacuo to give the title-compound. MS(ES) 460 [M+H]+

Provenance & Evidence