4-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic Acid → HCID 10118153, compound

Participants

Reaction Steps

N-[2-(4-Methoxy-3-sulphamoylphenyl)ethyl]-2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxylic acid and 5-(2-aminoethyl)-2-methoxybenzene-sulphonamide using method M. NMR; δH [2H6]—DMSO 8.66,(1H, t), 7.93-7.88,(3H, m), 7.76,(1H, d), 7.64,(1H, d), 7.54,(1H, d), 7.50,(2H, d), 7.45,(1H, dd), 7.14,(1H, d), 7.02,(2H, b), 3.86,(3H, s), 3.48,(2H, q), 2.85,(2H, t), 2.56,(3H, s), 2.31,(3H, s). LCMS; retention time 2.99 min, MH+ 507.

Provenance & Evidence