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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 131712Generated: November 1, 2026

3-Methylbenzylamine → HCID 10294228, compound

https://huagongshe.com/reaction/131712

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-MethylbenzylamineHCID 66015—
Reactant4-[2-methyl-5-(5-methyl-1,3,4-oxadiazol-2-yl)phenyl]benzoic AcidHCID 11220119—
ProductHCID 10294228HCID 10294228—

Reaction Steps

2′-Methyl-N-(3-methylbenzyl)-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxylic acid and 3-methylbenzylamine using method N. NMR; δH [2H6]—DMSO 9.11,(1H, t), 8.00,(2H, d), 7.90,(1H, dd), 7.77,(1H, d), 7.56-7.51,(3H, m), 7.21,(1H, t), 7.14-7.11,(2H, m), 7.05,(1H, d), 4.47,(2H, d), 2.56,(3H, s), 2.31, (3H, s), 2.29,(3H, s). LCMS; retention time 3.48 min, MH+ 398.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07384963B2
Source datasetuspto-grants-2008_06
ORD IDord-632f8d6d7be445d7b95e99b6913ade8c
Source noteuspto-grants-2008_06