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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 131731Generated: November 1, 2026

Methyl iodide → HCID 10112301, compound

https://huagongshe.com/reaction/131731

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 10294228HCID 10294228—
ProductHCID 10112301HCID 10112301—

Reaction Steps

2′-Methyl-N-methyl-N-(3-methylbenzyl)-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxamide was prepared from 2′-methyl-N-(3-methylbenzyl)-5′-(5-methyl-1,3,4-oxadiazol-2-yl)-1,1′-biphenyl-4-carboxamide and iodomethane using method L. NMR; δH [2H6]—DMSO 7.89,(1H, d), 7.76,(1H, s), 7.55-7.48,(5H, m), 7.27,(1H, t), 7.16-7.10,(2H, m), 7.00,(1H, b), 4.66-4.50,(2H, m), 2.89,(3H, m), 2.55,(3H, s), 2.32,(3H, s). LCMS; retention time 3.52 min, MH+ 412.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07384963B2
Source datasetuspto-grants-2008_06
ORD IDord-5a00cafabf284593a7a2d0b888735631
Source noteuspto-grants-2008_06