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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 132113Generated: October 28, 2026

tert-Butoxy bis(dimethylamino)methane → HCID 59733753, compound

https://huagongshe.com/reaction/132113

Reaction equation

Participants

RoleNameHCIDCharge
Reactanttert-Butoxy bis(dimethylamino)methaneHCID 79885—
ReactantHCID 59733726HCID 59733726—
SolventTolueneHCID 1140—
ProductHCID 59733753HCID 59733753—

Reaction Conditions

Temperature85 °C

Reaction Steps

To a stirred solution of tert-butyl 1-(3-tert-butylphenyl)-4-oxocyclohexylcarbamate (691 mg, 2.0 mmol) in Toluene (5 mL) was added tert-butoxybis(dimethylamino)methane (454 μL, 2.2 mmol). The reaction was stirred at 85° C. overnight. The reaction was concentrated and used crude in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07385085B2
Source datasetuspto-grants-2008_06
ORD IDord-c031964a759547a3b6ff31357bdf101f
Source noteuspto-grants-2008_06