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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 132515Generated: November 1, 2026

Chlorosuccinimide → HCID 136334118, compound

https://huagongshe.com/reaction/132515

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChlorosuccinimideHCID 31398—
ReactantHCID 135602108HCID 135602108—
SolventAcetic AcidHCID 176—
ProductHCID 136334118HCID 136334118—

Reaction Conditions

Temperature90 °C

Reaction Steps

A suspension of 3.0 g (13.09 mmol) of 2-(pyrimidin-4-yl)-6,7,8,9-tetrahydro-4H-pyrimido[1,2-a]pyrimidin-4-one in 60 ml of acetic acid was treated with 1.75 g (15.7 mmol) of N-chlorosuccinimide. The reaction mixture was heated at 90° C. during 18 h.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07388005B2
Source datasetuspto-grants-2008_06
ORD IDord-b869f96b244b44c3a8b7079841017ce2
Source noteuspto-grants-2008_06