HRID132760

反应详情

EQUATION

反应方程式

HRID 132760 的结构方程式

PROCEDURE

实验过程

Bornylamine (X) was recycled by first adjusting the pH of the aqueous solution of bornylamine-methane sulfonic acid (XM), obtained from the previous step, to 10-13, and then extracting the free amine into MTBE. After removal of solvent, 4.308 g of (R)-bornylamine (X) was obtained (>97% pure by 1H NMR, 92.6% yield).

WORKUP

后处理

  1. customobtained from the previous step, to 10-13
  2. extractionextracting the free amine into MTBE
  3. customAfter removal of solvent