HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1R,2S,4R)-Born-2-ylamine → (R)-bornylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1R,2S,4R)-Born-2-ylamine | HCID 32526 | — |
| Reactant | Bornylamine methane sulfonic acid | HCID 17950908 | — |
| Product | (R)-bornylamine | HCID 211083 | — |
Reaction Steps
Bornylamine (X) was recycled by first adjusting the pH of the aqueous solution of bornylamine-methane sulfonic acid (XM), obtained from the previous step, to 10-13, and then extracting the free amine into MTBE. After removal of solvent, 4.308 g of (R)-bornylamine (X) was obtained (>97% pure by 1H NMR, 92.6% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07388098B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-c0fd11cb5d4042c387c5853bf50515bc |
| Source note | uspto-grants-2008_06 |