Pyridine → HCID 69198227, compound

Participants

Reaction Steps

12.1 grams of ethyl 1-n-hexyl-2-hydroxy-cyclopentane carboxylate obtained in Example 17 were diluted with 60 ml of methylene chloride. At room temperature and with magnetic stirring, 6.108 ml of pyridine was slowly added, then 8.876 ml of benzoyl chloride was dropwise added. Then the procedure as described in Example 23 was followed, to give 18.16 g of yellow liquid. MS: 346(M+′), 345(M+−1), 301 (M+—OCH2CH3), 273(M+—CO2CH2CH3), 262, 241 (M+−C6H5CO), 225(M+—C6H5CO2), 195, 185, 151, 140, 105 (base), 77.

Provenance & Evidence