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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 132806Generated: November 2, 2026

Di-tert-butyl dicarbonate → HCID 67562678, compound

https://huagongshe.com/reaction/132806

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDi-tert-butyl dicarbonateHCID 90495—
Reactant1,2-Butanediol, 3-amino-4-(3,5-difluorophenyl)-, (2S,3S)-HCID 59734790—
SolventTetrahydrofuranHCID 8028—
ProductHCID 67562678HCID 67562678—

Reaction Steps

Aminodiol 27 was dissolved in THF and BOC2O was added and stirred overnight. Solvent removal afforded 28, which was carried directly into the next step; analytical sample m.p.=122°.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07388118B2
Source datasetuspto-grants-2008_06
ORD IDord-ac42f5607e114f48b21b8147b57a8f2c
Source noteuspto-grants-2008_06