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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 132852Generated: October 30, 2026

HCID 58687990, compound → HCID 69222706, compound

https://huagongshe.com/reaction/132852

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58687990HCID 58687990—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 69222706HCID 69222706—

Reaction Steps

To a solution of the compound from Step I above (1.25 g, 2.36 mmol) in absolute ethanol (100 mL) was added 10% palladium on carbon (480 mg). The reaction mixture was placed in a Parr apparatus and shaken under 50 psi of hydrogen for 4 hours. The solution was filtered through a pad of Celite and concentrated in vacuo to yield the title compound. LC/MS: 365 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07388019B2
Source datasetuspto-grants-2008_06
ORD IDord-608e0fd9976d4bd0b00f241b3933b2b9
Source noteuspto-grants-2008_06