HuagongsheHuagongshe Chemistry Print Report · For research reference only
6,7-Dihydro-2H-benzo[6,7]cyclohepta[cd]indazol-5-ylmethanol → 6,7-Dihydro-2H-benzo[6,7]cyclohepta[cd]indazole-5-carboxaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6,7-Dihydro-2H-benzo[6,7]cyclohepta[cd]indazol-5-ylmethanol | HCID 10125265 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Product | 6,7-Dihydro-2H-benzo[6,7]cyclohepta[cd]indazole-5-carboxaldehyde | HCID 10308069 | 100.8% |
Reaction Steps
120 mg of 6,7-dihydro-2H-benzo[6,7]cyclohepta[cd]indazol-5-ylmethanol prepared in Example 1-h was treated by the procedure of Example 1-f using 500 mg of manganese dioxide, to give 120 mg of the title compound as a colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07390797B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-c9c68d2d8e394311abcc1188ba2d05ef |
| Source note | uspto-grants-2008_06 |