HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17979845, compound → HCID 17979852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17979845 | HCID 17979845 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | MeOH tetrahydrofuran | HCID 21899815 | — |
| Product | HCID 17979852 | HCID 17979852 | 68.8% |
Reaction Steps
10 mg of palladium on charcoal (10% Pd) are added to a solution of 0.64 g of 2-amino-3-nitro-6-methoxyquinoline (compound B3) in 40 ml of methanol/tetrahydrofurane 1:1. After hydration for 0.5 h, the catalyst is filtered off and the filtrate is concentrated in vacuo. 0.38 g of the title compound are obtained as light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07390819B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-ed3ef764e67743d18213599cce8be5ee |
| Source note | uspto-grants-2008_06 |