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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 133091Generated: October 30, 2026

HCID 17979845, compound → HCID 17979852, compound

https://huagongshe.com/reaction/133091

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 17979845HCID 17979845—
CatalystPalladiumHCID 23938—
SolventMeOH tetrahydrofuranHCID 21899815—
ProductHCID 17979852HCID 1797985268.8%

Reaction Steps

10 mg of palladium on charcoal (10% Pd) are added to a solution of 0.64 g of 2-amino-3-nitro-6-methoxyquinoline (compound B3) in 40 ml of methanol/tetrahydrofurane 1:1. After hydration for 0.5 h, the catalyst is filtered off and the filtrate is concentrated in vacuo. 0.38 g of the title compound are obtained as light yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07390819B2
Source datasetuspto-grants-2008_06
ORD IDord-ed3ef764e67743d18213599cce8be5ee
Source noteuspto-grants-2008_06