Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 6-bromo-2-chloro-3-nitroquinoline | HCID 17979854 | — |
| Product | HCID 17979844 | HCID 17979844 | — |
Reaction Steps
0.8 g of 2-chloro-6-bromo-3-nitroquinoline (compound C4) are dissolved in 12 ml of ethanolic ammonia solution and stirred at 120° C. for 2.5 h in an autoclave. Under cooling in an ice bath, 0.55 g of the title compound precipitate from the reaction mixture as red crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07390819B2 |
|---|
| Source dataset | uspto-grants-2008_06 |
|---|
| ORD ID | ord-050668d0f5b345d4bf85526da67674ba |
|---|
| Source note | uspto-grants-2008_06 |
|---|
