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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 133791Generated: October 30, 2026

Trifluoroacetic acid → Trifluoroacetic acid

https://huagongshe.com/reaction/133791

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 86615410HCID 86615410—
SolventDichloromethaneHCID 6344—
ProductTrifluoroacetic acidHCID 6422—
ProductHCID 73320112HCID 73320112—

Reaction Steps

To a solution of tert-butyl 2-(4-acetamido-3,5-dichlorophenyl)-1-(3-(methoxyimino)-3-(4-methoxyphenyl)-propanamido)ethylidenecarbamate (12 mg) in dichloromethane (0.10 mL) was added TFA (0.10 mL), and the resulting mixture was stirred at room temperature for 12 h. The solvents were removed in vacuo to give the title compound as its TFA salt (10 mg). Retention time: 1.75 min (method A). MS (ESI) (M+H)+ 482.19.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07390925B2
Source datasetuspto-grants-2008_06
ORD IDord-ad41e7a820c846878685a87a3e3e3769
Source noteuspto-grants-2008_06