HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → Trifluoroacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86615410 | HCID 86615410 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 73320112 | HCID 73320112 | — |
Reaction Steps
To a solution of tert-butyl 2-(4-acetamido-3,5-dichlorophenyl)-1-(3-(methoxyimino)-3-(4-methoxyphenyl)-propanamido)ethylidenecarbamate (12 mg) in dichloromethane (0.10 mL) was added TFA (0.10 mL), and the resulting mixture was stirred at room temperature for 12 h. The solvents were removed in vacuo to give the title compound as its TFA salt (10 mg). Retention time: 1.75 min (method A). MS (ESI) (M+H)+ 482.19.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07390925B2 |
| Source dataset | uspto-grants-2008_06 |
| ORD ID | ord-ad41e7a820c846878685a87a3e3e3769 |
| Source note | uspto-grants-2008_06 |