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HRID13480

反应详情

EQUATION

反应方程式

HRID 13480 的结构方程式

REACTANTS

反应物

2
结构：C1COCCN1
HCID8083

Morpholine

C4H9NO

结构：O=[N+]([O-])c1ccc(CCBr)cc1
HCID79266

4-Nitrophenethyl bromide

C8H8BrNO2

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1ccc(CCN2CCOCC2)cc1
HCID2797473

4-[2-(4-nitrophenyl)ethyl]morpholine

C12H16N2O3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

To 4-(2-bromoethyl)-1-nitrobenzene (1 eq) in tetrahydrofuran was added morpholine (3 eq) and stir for 16 h at ambient temperature. Concentrating and passing through a plug of silica gave 4-[2-(4-nitrophenyl)ethylmorpholine. MS: MH+=236.

WORKUP

后处理

  1. concentrationConcentrating