Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 4-(3,5-diphenyl-4,5-dihydro-1H-pyrazol-1-yl)benzaldehyde | HCID 2792090 | — |
| Reactant | HCID 18458000 | HCID 18458000 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 73446797 | HCID 73446797 | — |
Reaction Steps
As shown in the following reaction 9, 0.5 g (2.5 mmol) of 2-(2-isopropyl-6-methyl-pyran-4-ylidene)-malononitrile and 0.815 g (2.5 mmol) of 4-(3,5-diphenyl-4,5-dihydro-pyrazol-1-yl)-benzaldehyde were added into 20 ml of ethanol, and 0.32 g (3.75 mmol) of piperidine was added thereto. The reaction solution was heated at 75° C. for 10 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07211335B2 |
|---|
| Source dataset | uspto-grants-2007_05 |
|---|
| ORD ID | ord-384fba05dab5467992f6cf3c3f64830d |
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| Source note | uspto-grants-2007_05 |
|---|
