HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 57617719, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | (S)-tert-Butyl (4-oxo-2,3,4,5-tetrahydrobenzo[b][1,4]oxazepin-3-yl)carbamate | HCID 18599719 | — |
| Product | HCID 57617719 | HCID 57617719 | — |
Reaction Steps
In an analogous manner to that described in example 5d), the alkylation by iodoethane of (S)-(8-oxo-6,7,8,9-tetrahydro-5-oxa-9-aza-benzocyclohepten-7-yl)-carbamic acid tert-butyl ester [Chem.Pharm.Bull. 1986, 34(3), 1128–47] yielded (87% of theory) the title compound as a white solid, m.p.: 112° C., MS m/e (%): 307.1 (M+H+, 93).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07211573B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-f2497da24ec44a7d82374b17da691dc5 |
| Source note | uspto-grants-2007_05 |