HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphoric Acid → HCID 67077056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | HCID 67076914 | HCID 67076914 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67077056 | HCID 67077056 | 81% |
Reaction Steps
The title compound was prepared in 81% yield by reaction of 460 mg (1.50 mmol) ((6R,7S)-6-ethyl-8-oxo-6,7,8,9-tetrahydro-5-oxa-9-aza-benzocyclohepten-7-yl)-carbamic acid tert-butyl ester with 2.23 g (22.5 mmol) ortho phosphoric acid in 4 ml tetrahydrofurane, MS m/e (%): 207.1 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07211573B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-88a35be08be443e4bb609f12e7605c3e |
| Source note | uspto-grants-2007_05 |