HRID1348652

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6422

未命名化合物

结构：C[C@H]1Oc2ccc(F)cc2N(CC(F)(F)F)C(=O)[C@H]1NC(=O)OC(C)(C)C

HCID67077130

未命名化合物

PRODUCTS

生成物

结构：C[C@H]1Oc2ccc(F)cc2N(CC(F)(F)F)C(=O)[C@H]1N

HCID21091439

未命名化合物

收率 75%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The title compound was prepared in 75% yield by reaction of 3.70 g (9.0 mmol) [(6R,7S)-2-fluoro-6-methyl-8-oxo-9-(2,2,2-trifluoro-ethyl)-6,7,8,9-tetrahydro-5-oxa-9-aza-benzocyclohepten-7-yl]-carbamic acid tert-butyl ester with 18 ml trifluoroacetic acid in 75 ml dichloromethane, MS m/e (%): 293.1 (M+H+, 100).