1-Methylpiperazine → HCID 67213406, compound

HRID 1348713Notes

Reaction equation

HRID 1348713 reaction equation
[CH2:1]([N:5]1[C:10](=[O:11])[C:9]([CH2:12]OS(C)(=O)=O)=[CH:8][C:7]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[N:6]1)[CH:2]([CH3:4])[CH3:3].[CH3:24][N:25]1[CH2:30][CH2:29][NH:28][CH2:27][CH2:26]1>>[CH2:1]([N:5]1[C:10](=[O:11])[C:9]([CH2:12][N:28]2[CH2:29][CH2:30][N:25]([CH3:24])[CH2:26][CH2:27]2)=[CH:8][C:7]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[N:6]1)[CH:2]([CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 531671-MethylpiperazineHCID 219915622-isobutyl-4-methanesulfonyloxymethyl-6-phenyl-2H-pyridazin-3-one

Product 1

HCID 67213406HCID 67213406, compoundYield 77.1%

Procedure

Following the procedure of Example 1(10), 2-isobutyl-4-methanesulfonyloxymethyl-6-phenyl-2H-pyridazin-3-one and N-methylpiperazine were reacted to yield the title compound as a yellow oil (yield: 77.1%).

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-9743c09d768a4396b031f4ebc6915cc0
Source dataset
uspto-grants-2007_05
Patent number
US07211577B2

Reaction notes

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