HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → HCID 69250511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | 4-Phenylbenzoyl chloride | HCID 84151 | — |
| Reactant | (2S)-1-((tert-butoxy)carbonyl)-4-methylidenepyrrolidine-2-carboxylic acid | HCID 21727417 | — |
| Product | HCID 69250511 | HCID 69250511 | — |
Reaction Steps
Following the general method as outlined in Example 22, starting from 1-(tert-butoxycarbonyl)-4-methyleneproline, [1,1′-biphenyl]-4-carbonyl chloride, and 1,2-benzenedi-amine the title compound was obtained in 73% purity by LC/MS. MS(ESI+): m/z=380.4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07211601B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-9bb5911dfdd7422cb01b5b60411ff09b |
| Source note | uspto-grants-2007_05 |