Furfurylamine → HCID 69247854, compound

HRID 1349218Notes

Reaction equation

HRID 1349218 reaction equation
C(O[C:6]([N:8]1[CH2:15][C:14](=[CH2:16])[CH2:13][C@H:9]1[C:10]([OH:12])=O)=[O:7])(C)(C)C.[N:17]([C:20]1[CH:25]=[CH:24][CH:23]=[C:22]([O:26][CH3:27])[CH:21]=1)=C=O.[O:28]1[CH:32]=[CH:31][CH:30]=[C:29]1[CH2:33][NH2:34]>>[O:28]1[CH:32]=[CH:31][CH:30]=[C:29]1[CH2:33][NH:34][C:10]([C@@H:9]1[CH2:13][C:14](=[CH2:16])[CH2:15][N:8]1[C:6]([NH:17][C:20]1[CH:25]=[CH:24][CH:23]=[C:22]([O:26][CH3:27])[CH:21]=1)=[O:7])=[O:12]

Participants

4

Reactant 3

HCID 3438FurfurylamineHCID 878433-Methoxyphenyl isocyanateHCID 21727417(2S)-1-((tert-butoxy)carbonyl)-4-methylidenepyrrolidine-2-carboxylic acid

Product 1

HCID 69247854HCID 69247854, compound

Procedure

Following the general method as outlined in Example 22, starting from 1-(tert-butoxycarbonyl)-4-methyleneproline, 1-isocyanato-3-methoxybenzene, and 2-furylmethylamine the title compound was obtained in 95% purity by LC/MS. MS(ESI+): m/z=356.0.

Sources & evidence

ORD record
ord-3358c137520e4c89a2c8af26f65c496e
Source dataset
uspto-grants-2007_05
Patent number
US07211601B2

Reaction notes

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