HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Aminomethyl)cyclohexan-1-ol → HCID 131726383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Aminomethyl)cyclohexan-1-ol | HCID 77614 | — |
| Reactant | 4-Pyridin-3-yl-benzoic acid | HCID 1515244 | — |
| Reactant | (2S,4EZ)-1(tert-butoxycarbonyl)-4-(methoxyimino)-2-pyrrolidinecarboxylic acid | HCID 58714586 | — |
| Product | HCID 131726383 | HCID 131726383 | — |
Reaction Steps
Following the general method as outlined in Example 22, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-(methoxyimino)-2-pyrrolidinecarboxylic acid, 4-(3-pyridinyl)benzoic acid, and 1-(aminomethyl)cyclohexanol, the title compound was obtained in 69% purity by HPLC. MS(ESI+): m/z=451.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07211601B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-b390fbf2397f4c2483342f7fbe29726c |
| Source note | uspto-grants-2007_05 |