HCID 12988737, compound → HCID 12988738, compound

Participants

Reaction Steps

The compound obtained in Example 1 (54 mmol), in the form of a base, is dissolved in 50 ml of methanol and then palladium-on-carbon (150 mg) is added to the solution. The reaction mixture is stirred at ambient temperature and under hydrogen for 4 hours. After removal of the palladium-on-carbon by filtration, the organic phase is evaporated under reduced pressure. The oil obtained is purified by chromatography on silica gel to yield the title product in the form of a yellow oil.

Provenance & Evidence