HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21093530, compound → (S)-2-Isopropyl-10-{3-[2-(4-methoxy-phenyl)-ethyl]-piperazin-1-yl}-4H-3-thia-1,4,9-triaza-benzo[f]azulene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21093530 | HCID 21093530 | — |
| Reactant | 2-isopropyl-4H-3-thia-1,4,9-triaza-benzo[f]azulen-10-ylamine | HCID 135797740 | — |
| Product | (S)-2-Isopropyl-10-{3-[2-(4-methoxy-phenyl)-ethyl]-piperazin-1-yl}-4H-3-thia-1,4,9-triaza-benzo[f]azulene | HCID 136005625 | 38.4% |
Reaction Steps
By using a similar method of the method of Example 460, using 2-isopropyl-4H-3-thia-1,4,9-triaza-benzo[f]azulen-10-ylamine(1.48 g, 5.7 mmol) and (S)-2-[2-(4-methoxy-phenyl)-ethyl]-piperazine (1.26 g, 5.7 mmol) to give 1.01 g of the title compound as a yellow solid: mass spectrum (ion spray): m/z=462 (M+1); Analysis for C26H31N5OS(0.3 H2O): calcd: C, 66.87; H, 6.82; N, 15.00; found: C, 66.58; H, 6.35; N, 14.96.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07214673B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-ff9dbfdab0a1452095e857d8496b3a70 |
| Source note | uspto-grants-2007_05 |