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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1350574Generated: October 31, 2026

Ammonia → HCID 58861252, compound

https://huagongshe.com/reaction/1350574

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantHCID 21096966HCID 21096966—
SolventMethanolHCID 887—
ProductHCID 58861252HCID 58861252—

Reaction Steps

The process is performed according to the procedure described in Example 3 (step 3.4). Starting with 1.28 g (3.42 mmol) of 3-{2-[1-(6-chloro-2-quinolyl)-4-piperidyl]ethyl}-1,3-oxazolidine-2,4-dione, obtained in step 10.3, and 22.10 ml (154.08 mmol) of a solution (7M) of aqueous ammonia in methanol, and after crystallization from ethanol, 0.64 g of pure product is obtained in the form of a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07214798B2
Source datasetuspto-grants-2007_05
ORD IDord-f90413af9eeb4e11ba0224490c759a78
Source noteuspto-grants-2007_05