HRID13506

反应详情

EQUATION

反应方程式

HRID 13506 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Chloro-5-nitropyridine (1.0 eq) and dimethylamine (2 M in EtOH, 4.6 eq) in NMP were heated for 2 h at 100° C. The solution was then poured slowly into H2O. The filtrate that formed was filtered and dried to give 2-(dimethylamino)-5-nitropyridine.

WORKUP

后处理

  1. customThe filtrate that formed
  2. filtrationwas filtered
  3. customdried