HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Azido-4-methylbenzoic acid → 3-Azido-N-(5-tert-butyl-3-cyano-2-methoxy-phenyl)-4-methyl-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Azido-4-methylbenzoic acid | HCID 17973091 | — |
| Reactant | 3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide | HCID 21079202 | — |
| Reactant | 3-Amino-5-(tert-butyl)-2-methoxybenzonitrile | HCID 21097297 | — |
| Product | 3-Azido-N-(5-tert-butyl-3-cyano-2-methoxy-phenyl)-4-methyl-benzamide | HCID 21097302 | — |
Reaction Steps
3-Azido-N-(5-tert-butyl-3-cyano-2-methoxy-phenyl)-4-methyl-benzamide was prepared from 3-azido-4-methyl benzoic acid (U.S. Ser. No. 04/102,492) and 3-amino-5-tert-butyl-2-methoxy-benzonitrile in the same manner as 3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide (Example 15).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07214802B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-b8fa7c4a6ee24560ab3187e734d98d6a |
| Source note | uspto-grants-2007_05 |