HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21097609, compound → HCID 21097608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21097609 | HCID 21097609 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic acid ethanol | HCID 18476134 | — |
| Product | HCID 21097608 | HCID 21097608 | 95% |
Reaction Steps
A stirred solution of the product of step (b) (0.97 g) and 10% palladium on carbon (100 mg) in acetic acid:ethanol (1:9, 20 mL) was placed under an atmosphere of hydrogen at 20° C. for 2 hours. The reaction mixture was filtered through a pad of celite and the solvent was removed in vacuo to give the title compound (780 mg). LC retention time 2.45 mins
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07217409B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-c4496e39d71d41abbbdc4d4be4a88fa1 |
| Source note | uspto-grants-2007_05 |