HCID 21098149, compound → HCID 21098099, compound

HRID 1351080Notes

Reaction equation

HRID 1351080 reaction equation
[CH3:1][C:2]1[C:11]([CH3:12])=[N:10][C:9]2[C:4](=[C:5]([CH3:17])[CH:6]=[C:7]([C:13](OC)=[O:14])[CH:8]=2)[N:3]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[CH3:1][C:2]1[C:11]([CH3:12])=[N:10][C:9]2[C:4](=[C:5]([CH3:17])[CH:6]=[C:7]([CH2:13][OH:14])[CH:8]=2)[N:3]=1

Participants

4

Reactant 2

HCID 21098149HCID 21098149, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 21098099HCID 21098099, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Prepared by reducing 691 mg of methyl 2,3,8-trimethyl-quinoxaline-6-carboxylate with 300 mg of lithium aluminium hydride (95%) in 15 ml tetrahydrofuran at ambient temperature.

Workup

  1. customPrepared
  2. customat ambient temperature

Sources & evidence

ORD record
ord-326e2e6e619c403b8a44ca178164fab5
Source dataset
uspto-grants-2007_05
Patent number
US07217711B2

Reaction notes

Loading…