HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methyl-2-(pyridin-3-YL)ethanamine → 7-Oxo-4,5,6,7-tetrahydro-benzo[b]thiophene-3-sulfonic acid methyl-(2-pyridine-3-vi-ethyl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methyl-2-(pyridin-3-YL)ethanamine | HCID 5152594 | — |
| Reactant | 7-Oxo-4,5,6,7-tetrahydrobenzo[b]thiophene-3-sulfonyl chloride | HCID 21098685 | — |
| Product | 7-Oxo-4,5,6,7-tetrahydro-benzo[b]thiophene-3-sulfonic acid methyl-(2-pyridine-3-vi-ethyl)-amide | HCID 69416662 | — |
Reaction Steps
From methyl-(2-pyridine-3-yl-ethyl)-amine (the compound of Preparation Example 15) (82 mg) and 7-oxo-4,5,6,7-tetrahydro-benzo-[b]thiophene-3-sulfonyl chloride (the compound of Preparation Example 7) (150 mg), the title compound (138 mg) was obtained as a colorless oily matter, in the same way as Preparation Example 41.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07217723B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-f3d2a7536dc940e08028cb717969c2a6 |
| Source note | uspto-grants-2007_05 |