HRID1351334

反应详情

EQUATION

反应方程式

HRID 1351334 的结构方程式

PROCEDURE

实验过程

3-Methyl-3-phenyl-pyrrolidine, which was synthesized by reducing 3-methyl-3-phenyl pyrrolidine-2,5-dione with aluminum lithium hydride, was used as the amine to carry out the reaction according to <method α>. A purification by silica gel column chromatography (hexane/ethyl acetate) was carried out, and, the title compound (7 mg) was obtained as a colorless solid.

WORKUP

后处理

  1. customA purification by silica gel column chromatography (hexane/ethyl acetate)