HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 69040905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 21099367 | HCID 21099367 | — |
| Product | HCID 69040905 | HCID 69040905 | — |
Reaction Steps
N-Boc-L-proline 4-nitrooxybutyl ester (1.24 g, 3.7 mmol) was dissolved in CH2Cl2 (20 mL) and HCl gas was bubbled into the solution for 2 hours. Then the mixture was concentrated, affording L-proline 4-nitrooxybutyl ester hydrochloride as a clear oil (1.00 g, quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07217733B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-ad4cac4e5d9d49d58399624364e8e53c |
| Source note | uspto-grants-2007_05 |