HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Dimethyl-1-butanol → 3,3-Dimethyl-1-butyl 5-amino-4-oxopentanoate Hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Dimethyl-1-butanol | HCID 12233 | — |
| Reactant | Aminolevulinic Acid Hydrochloride | HCID 123608 | — |
| Product | 3,3-Dimethyl-1-butyl 5-amino-4-oxopentanoate Hydrochloride | HCID 57438253 | — |
Reaction Steps
From 3,3-dimethyl-1-butanol (5.0 g; 49 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol) at 70° C. The reaction was complete after 4 h. The yield was 0.91 g (60%), mp146–148°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07217736B2 |
| Source dataset | uspto-grants-2007_05 |
| ORD ID | ord-dbc3cf343c5c497bb66d269b56055d91 |
| Source note | uspto-grants-2007_05 |